Item | Specifications | Results |
Appearance | White or slightly yellow,crystalline powder | Conform |
Solubility | Practically insoluble in water,soluble in dimethylformamide,sparingly soluble in ethanol and in methylene chloride. It dissolves in dilute solutions of alkali hydroxides. | Conform |
Identification |
| 1.2 Conform Conform |
Melting point | About 213.0ºC | 212.0-212.7 |
Related substances | Impurity A<0.1%;impurity B<0.05% | Conform |
Any other impurity <0.1% | ||
Total impurity<0.5% | ||
Copper | Not more than 10ppm | Conform |
Loss on drying | Not more than 0.5% | 0.2% |
Sulphated ash | Not more than 0.1% | <0.1% |
Assay (basis on dry) | 99.0%~101.0% | 99.6% |
Conclusion | The results conforms with BP2009/USP23 standards |